ЯМР для продуктов гидроформилирования

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Ищу ЯМР описание для продуктов гидроформилирования гептена-1 и октена-1, т.е. линейного (октаналь и нонаналь) и разветвленного (2-метилгептаналь и 2-метилоктаналь) альдегидов. Может у кого есть эти данные. Продукты и исходник можно идентифицировать, но хотел бы ссылки. Поиск в дурном reaxys не дал ничего.

[gugu]

В олдричевской базе данных смотрели?

[suprachemister]

еще варианты: SpecInfo (Wiley),
SciFinder:
Octanal
Spectra Properties Value Condition Note
Carbon-13 NMR Spectrum See spectrum (36) WSS
Carbon-13 NMR Spectrum See spectrum (37) AIST
Carbon-13 NMR Spectrum See full text 1 of 14 (38) CAS
Proton NMR Spectrum See spectrum (37) AIST
Proton NMR Spectrum See full text 1 of 23 (52) CAS
(36) WSS: Spectral data were obtained from Wiley Subscription Services, Inc. (US)
(37) AIST: Integrated Spectral Database System of Organic Compounds. (Data were obtained from the National Institute of Advanced Industrial Science and Technology (Japan))
(38) Jiang, Nan; Organic Letters 2005, V7(17), P3689-3692 CAPLUS
(52) Rolfe, Alan; Journal of Organic Chemistry 2008, V73(22), P8785-8790 CAPLUS


Nonanal
Spectra Properties Value Condition Note
Carbon-13 NMR Spectrum See spectrum (32) WSS
Carbon-13 NMR Spectrum See spectrum (33) AIST
Carbon-13 NMR Spectrum See full text (34) CAS
Carbon-13 NMR Spectrum See full text (35) CAS
Carbon-13 NMR Spectrum See full text (36) CAS
Carbon-13 NMR Spectrum See full text (37) CAS
Proton NMR Spectrum See spectrum (33) AIST
Proton NMR Spectrum See full text (34) CAS
Proton NMR Spectrum See full text (36) CAS
Proton NMR Spectrum See full text (35) CAS
Proton NMR Spectrum See full text (37) CAS
Proton NMR Spectrum See full text (64) CAS
Proton NMR Spectrum See full text (14) IC
Proton NMR Spectrum See full text (65) CAS
Proton NMR Spectrum See full text (66) CAS
Proton NMR Spectrum See full text (67) IC
(32) WSS: Spectral data were obtained from Wiley Subscription Services, Inc. (US)
(33) AIST: Integrated Spectral Database System of Organic Compounds. (Data were obtained from the National Institute of Advanced Industrial Science and Technology (Japan))
(34) Ricken, Stefan; Journal of Molecular Catalysis A: Chemical 2006, V257(1-2), P78-88 CAPLUS
(35) Layek, Keya; Advanced Synthesis & Catalysis 2011, V353(4), P606-616 CAPLUS
(36) Makado, Gouki; Advanced Synthesis & Catalysis 2010, V352(2+3), P299-304 CAPLUS
(37) Akkilagunta, Vijay Kumar; Synlett 2010, (17), P2571-2574 CAPLUS
(64) Schwartz, Chris; Organic Letters 2006, V8(15), P3199-3201 CAPLUS
(65) Petricci, Elena; Organic Letters 2006, V8(17), P3725-3727 CAPLUS
(66) Wertz, Sebastian; Advanced Synthesis & Catalysis 2011, V353(1), P69-72 CAPLUS
(67) Huang, Xian; Youji Huaxue 1986, (3), P204-6 CAPLUS
(14) Tanaka, Kazuhiko; Bulletin of the Chemical Society of Japan 1980, V53(12), P3619-22 CAPLUS

2-Methylheptanal
Spectra Properties Value Condition Note
Proton NMR Spectrum See full text (5) IC
Proton NMR Spectrum See full text (3) CAS
(1) Thoms, H.; Archiv der Pharmazie und Berichte der Deutschen Pharmazeutischen Gesellschaft 1925, V263, P241-52 CAPLUS
(2) GB 808880 1959 CAPLUS
(3) Sheng, Shou-Ri; Synthetic Communications 2006, V36(4), P429-434 CAPLUS
(4) WSS: Spectral data were obtained from Wiley Subscription Services, Inc. (US)
(5) Chuit, C.; Tetrahedron 1980, V36(16), P2305-10 CAPLUS



2-Methyloctanal
Spectra Properties Value Condition Note
Carbon-13 NMR Spectrum See spectrum (3) WSS
Carbon-13 NMR Spectrum See full text (4) CAS
Carbon-13 NMR Spectrum See full text (5) CAS
Proton NMR Spectrum See full text (5) CAS
Proton NMR Spectrum See full text (4) CAS
Proton NMR Spectrum See full text (1) IC
Proton NMR Spectrum See full text (7) IC
(1) Syper, Ludwik; Tetrahedron 1987, V43(12), P2853-71 CAPLUS
(2) Kulesza, Janusz; Riechstoffe, Aromen, Koerperpflegemittel 1969, V19(1), P8,10,12 CAPLUS
(3) WSS: Spectral data were obtained from Wiley Subscription Services, Inc. (US)
(4) Ricken, Stefan; Journal of Molecular Catalysis A: Chemical 2006, V257(1-2), P78-88 CAPLUS
(5) Makado, Gouki; Advanced Synthesis & Catalysis 2010, V352(2+3), P299-304 CAPLUS
(6) Zope, Dhananjay D.; Indian Perfumer 2008, V52(1), P60-62 CAPLUS
(7) Duchene, Alain; Bulletin de la Societe Chimique de France 1985, (5), P787-93 CAPLUS

spectra11.rar

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