1. The collapse temperature in freeze drying: Dependence on measurement methodology and rate of water removal from the glassy phase
Michael J. Pikal, a and Saroj Shah
International Journal of Pharmaceutics Volume 62, Issues 2-3, 31 July 1990, Pages 165-186
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http://dx.doi.org/10.1016/0378-5173(90)90231-RDouglas R. Macfarlane
Cryobiology Volume 23, Issue 3, June 1986, Pages 230-244
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http://dx.doi.org/10.1016/0011-2240(86)90049-03. Use of subambient thermal analysis to optimize protein lyophilization
Byeong S. Chang1 and Cynthia S. Randall
Cryobiology Volume 29, Issue 5, October 1992, Pages 632-656
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http://dx.doi.org/10.1016/0011-2240(92)90067-C