+++поиск в Reaxys/SF

[Indazole]

Здравствуйте!
Посмотрите, пожалуйста, свойства и методы получения для:

InChI Key:
NRXYBKZDRCXDOD-SNVBAGLBSA-N

и

InChI Key:
NEZIIRPIEDUFFK-FRRDWIJNSA-N

[mishka]

получение только для 1

Lee; Long; Murray; Adams; Nuttall; Nadeau; Kikly; (…)Keller; DeWolf Jr.
Journal of Medicinal Chemistry, 2001, vol. 44, # 12, p. 2015 - 2026


Chen, Rui-Jia; Wang, Jun-Jie; Han, Li; Gu, Yu-Cheng; Xu, Zhi-Ping; Cheng, Jia-Gao; Shao, Xu-Sheng; Xu, Xiao-Yong; Li, Zhong
Journal of Heterocyclic Chemistry, 2021, vol. 58, # 7, p. 1429 - 1436



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Current Patent Assignee: SELABTEC SCIENCES SLU - WO2024/83861, 2024, A1
Location in patent: Page/Page column 25; 28

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Coldham, Iain; Dufour, Samuel; Haxell, Thomas F. N.; Patel, Jignesh J.; Sanchez-Jimenez, Graciela
Journal of the American Chemical Society, 2006, vol. 128, # 33, p. 10943 - 10951
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Current Patent Assignee: SMITHKLINE BEECHAM - US6403792, 2002, B1

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спктры для первого
ПМР
Lee; Long; Murray; Adams; Nuttall; Nadeau; Kikly; (…)Keller; DeWolf Jr.
Journal of Medicinal Chemistry, 2001, vol. 44, # 12, p. 2015 - 2026

масс

Current Patent Assignee: SMITHKLINE BEECHAM - US6403792, 2002, B1


HPLC (High performance liquid chromatography)
supporting information
Cao, Lei; Zhang, Xing-Ping; Xie, Ming-Sheng; Guo, Hai-Ming
Journal of Organic Chemistry, 2023, vol. 88, # 1, p. 341 - 346

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для 2-го

ЯМР, IR Spectroscopy, масс

Almasi, Diana; Alonso, Diego A.; Gomez-Bengoa, Enrique; Nagel, Yvonne; Najera, Carmen
European Journal of Organic Chemistry, 2007, # 14, p. 2328 - 2343


Melting Point, °C Solvent (Melting Point) Reference
169
ethyl acetate, methanol
Almasi, Diana; Alonso, Diego A.; Gomez-Bengoa, Enrique; Nagel, Yvonne; Najera, Carmen
European Journal of Organic Chemistry, 2007, # 14, p. 2328 - 2343

Optical Rotatory Power - 1
Show/Hide columns
Type (Optical Rotatory Power) Concentration (Optical Rotatory Power) Solvent (Optical Rotatory Power) Optical Rotatory Power, deg Wavelength (Optical Rotatory Power), nm Temperature (Optical Rotatory Power), °C Reference
[alpha]
1.0 g/100ml
CH2Cl2
24.6
589
20
Almasi, Diana; Alonso, Diego A.; Gomez-Bengoa, Enrique; Nagel, Yvonne; Najera, Carmen
European Journal of Organic Chemistry, 2007, # 14, p. 2328 - 2343

[Indazole]

Спасибо!